An Two-Step Experiment Process to Synthesize N, N-Diethyl-M-Toluamide (905 words, 4 pages)
N,N-Diethyl-m-ToluamideObjective to synthesize N,N-diethyl-m-toluamide in a two-step process involving m-toluic acid, thionyl chloride, and diethylamineReactionsTable of ReagentsProductsReagent 1Reagent 2Reagent 3Solvent 1Product 1NameM-toluic acidThionyl chlorideDiethylamineAnhydrous etherN-N-diethyl-m-toluamideFormulaC8H8O2SOCl2C4H11NC4H10OC12H17NOMolecular Weight136.15 gmol118.97 gmol73.14 gmol74.12 gmol191.27 gmolDensity1.05 gcm31.638 gcm30.7074 gmL0.713 gcm30.998 gmLQuantity (g, mL)0.273g0.30 mL0.66 mLsolvent (various amounts)0.012Millimoles2.00 mmol4.1 mmol6.4 mmolna0.627 mmolEquivalents1.02.13.2na0.031Experimental procedureM-toluic acid, a flaky ...
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